Re: carbon-13 NMR

hendrycl@plu.edu
Mon, 17 Mar 1997 17:26:31 -0800 (PST)

Has anyone else been having problems with posting emails to the TOJC
archives?... (I'm writing this message for the second time because it
didn't go through the first time).

I wanted to find out how other people interpreted their NMR spectra. Dr.
Fryhle mentioned that we were not to worry about the s, d, t, and q
designations to the C-13 NMR spectra in the book. I used these as part of
my interpretation-- for example a singlet C (as Gabe defined) is part of a
carbonyl group in the carvone molecule. I therefore labeled the "s" peak
in the "ketone" region of the spectra with a letter and labeled the
corresponding carbon in the molecular representation with that same
letter. I also saw that there were two singlet peaks in the alkene region
of the spectra so I labled those two peaks and the two singlet carbons in
the molecule that were part of C-C double bonds with corresponding
letters. I used the s, d, t, and q designations from the book but used the
NMR spectra from the lab window...

chase

On Mon, 17 Mar 1997, Gabriel D. Charbonneau wrote:

> Terra,
> I know Dr. Fryhle said that we don't need to know what singlets,
> doublets, triplets, and quartets are, but Chason and I spent a long time
> figuring it out and I just thought I would share with inquiring minds. A
> peak that is a singlet is representing a carbon in the structure that has
> no hydrogens attached to it. A doublet represents a carbon with one
> hydrogen attached, a triplet is a carbon with two hydrogens, and a quartet
> is one with three. The designations singlet, doublet, etc... refer to the
> number of nuclei ie. A doublet represents two nuclei: one carbon and
> one hydrogen.
> For an example of how this is useful in interpreting NMR spectra
> look at the figure on page 117 Pavia et al. The two quartets represent
> the two CH3 groups in the carvone molecule.
>
> Gabe
>
> On Mon, 17 Mar 1997 bobbtl@plu.edu wrote:
>
> > In the NMR spectrum of carvone on pg. 117 of Pavia et al, what does the
> > s=singlet, d=doublet, t=triplet, q=quartet refer to exactly and should
> > this be taken into consideration when labeling our spectrum?
> >
> > Terra
> >
> >
>
>